INTERACTIVE INSTRUCTIONAL TEXT 
A Project by Professors Chickos, Garin and D'Souza


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The authors have attempted to deliver an accurate copy of the organic laboratory manual and to verify that the information and data contained therein have been selected on the basis of sound scientific judgment. However, the University of Missouri-St. Louis makes no warranties to that effect, and shall not be liable for any damage that may result from errors or omissions in the manual. Feel free to edit the downloadable version of this document as you choose, but read and accept the "disclaimer" added at the suggestion of the university lawyer given below. Please acknowledge the authors and the UM-St. Louis Chemistry Department if you use any of this material but clearly indicate if any modifications have been made from the original. Please contact us at orglab@jinx.umsl.edu if you use or modify the text. We would be happy to link your website to ours for access to any modifications you incorporate into the document. 


Disclaimer

"These experiments are designed to be used in college and university level chemistry laboratory courses, and should not be conducted unless there is an appropriate level of supervision, safety training, personal protective equipment and other safety facilities available for users.  Any users of these procedures assume all responsibility for the safe handling of hazardous chemicals and procedures. The Curators of the University of Missouri, a public corporation, its officers, employees and agents shall not be liable for any damages in connection with, or arising out of, the furnishing, performance, or use of these procedures.  The Curators of the University of Missouri, a public corporation, its officers, employees and agents make no warranties, express or implied, as to results to be obtained from the information presented.

Users may reprint this information, on the condition that full attribution is given to the authors and the University of Missouri-St. Louis. Users may not revise, modify or edit this information without the permission of the authors and the University of Missouri-St. Louis except for use by qualified instructors in an organic chemistry laboratory course at an institution for higher education."




 

Lab Manual

Syllabus (Word file) (Pdf file)
Introduction (Word file) (Pdf file)

Discussions

Safety  (Word file) (Pdf file)
Notebook  (Word file) (Pdf file)
Glassware and Equipment (Word file) (Pdf file)
Common Laboratory Techniques (Word file) (Pdf file)
Distillation (Word file)  (Pdf file)
Infrared Spectroscopy (Word file)  (Pdf file)
Revised Infrared Spectroscopy (Word file)  (Pdf file)
IR Spectra of Selected Compounds (Word file)  (Pdf file)

Experiments

Experiment 1 - Synthesis of Aspirin   (Word file) (Pdf file)
Experiment 2 - Synthesis of Acetaminophen   (Word file) (Pdf file)
Experiment 3 - Extraction of Caffeine   (Word file) (Pdf file)
Experiment 4 - Thin Layer Chromatography (TLC)    (Word file) (Pdf file)
Experiment 5 - Synthesis of Isopentyl Acetate (Banana Oil)   (Word file) (Pdf file)
Experiment 6 - Steam Distillation of Methyl Salicylate, Hydrolysis of an Ester    (Word file) (Pdf file)
Experiment 7 - Distillation of a Mixture    (Word file) (Pdf file)
Experiment 8 - Identification of Unknowns   (Word file) (Pdf file)
Experiment 9 - Multistep Synthesis   (Word file) (Pdf file)

Appendix

Tables of Selected Unknowns and Derivatives